Atomic Force Microscope (AFM)

AFMAtomic force microscopy (AFM) is a method of measuring surface topography on a scale from angstroms to 100 microns. The technique involves imaging a sample through the use of a probe, or tip, with a radius of 20 nm. The tip is held several nanometers above the surface using a feedback mechanism that measures surface–tip interactions on the scale of nanoNewtons. Variations in tip height are recorded while the tip is scanned repeatedly across the sample, producing a topographic image of the surface.

In addition to basic AFM, the instrument in the Microscopy Suite is capable of producing images in a number of other modes, including tapping, magnetic force, electrical force, and pulsed force. In tapping mode, the tip is oscillated above the sample surface, and data may be collected from interactions with surface topography, stiffness, and adhesion. This results in an expanded number of image contrast methods compared to basic AFM. Magnetic force mode imaging utilizes a magnetic tip to enable the visualization of magnetic domains on the sample. In electrical force mode imaging a charged tip is used to locate and record variations in surface charge. In pulsed force mode (Witec), the sample is oscillated beneath the tip, and a series of pseudo force-distance curves are generated. This permits the separation of sample topography, stiffness, and adhesion values, producing three independent images, or three individual sets of data, simultaneously.

This instrument may also be used with a scanning tunnelling microscope (STM) head. STM utilizes quantum mechanical tunnelling of electrons to image conducting surfaces. 

ITG users may reserve time on the AFM using the AFM calendar.

Manufacturer: Digital Instruments
Equipment Model: Multimode NanoScope IIIa
Features: capable of contact, tapping, magnetic force, electric force, and phase imaging modes; J-scanner with an x,y range of 125 microns and a vertical range of 5 microns; A-scanner with an x,y range of 1 micron and a vertical range of 400 nm; analyses may be performed in air or liquid cell; scanning tunnelling microscopy (STM) head
- Pulsed force mode
Location: B606G
Contact Person: Leilei Yin
Contact Information: Microscopy Suite Staff:
Leilei Yin  (217) 265-0875

Digital Instruments Help Desk:
1-800-873-9750
Fees & Consumables: See Microscopy Suite Fees & Consumables
Related Forums: Probing Polymer Subsurface Structure Using Tapping Mode Atomic Force Microscopy.
Measuring Surface Adhesion and Stiffness on the Nanometer Scale Using Pulsed-Force Microscopy.
Magnetic and Electronic Force Microscopy using the AFM.
Introduction to Atomic Force Microscopy.
Related Technical reports: Imaging Electrochemical Controlled Chemical Gradients Using Pulsed Force Mode Atomic Force Microscopy.
File Format: AFM files have a proprietary format and can be viewed with the Digital Instruments software or Image SXM. They can also be saved from the Digital Instruments software into other formats, such as tiff.